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'''Field emission microscopy''' (FEM) is an analytical technique used in [[materials science]] to investigate molecular surface structures and their electronic properties.<ref>{{cite web | title = Intro to Field Emission  | publisher = Field Emission / Ion Microscopy Laboratory, Purdue University, Dept. of Physics | url = http://physics.unipune.ernet.in/~fem/intro-fem.htm | accessdate = 2007-05-10}}</ref> Invented by [[Erwin Wilhelm Müller]] in 1936, the  FEM was one of the first surface analysis instruments that approached near-[[Atom|atomic]] [[Optical resolution|resolution]].
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==Introduction==
Microscopy techniques are used to produce real space magnified images of a surface showing what it looks like. In general microscopy information concerns surface [[crystallography]] (i.e. how the atoms are arranged at the surface), surface morphology (i.e. the shape and size of topographic features making the surface), and surface composition (the elements and compounds the surface is composed of).
 
Field emission microscopy (FEM) was invented by Erwin Müller in 1936. In FEM, the phenomenon of [[field electron emission]] was used to obtain an image on the detector on the basis of the difference in work function of the various crystallographic planes on the surface.
 
==Design==
A Field Emission Microscope consists of a metallic sample in the form of a sharp tip and a conducting fluorescent screen enclosed in ultrahigh vacuum. The tip radius used is typically of the order of 100 nm. It is composed of a metal with a high [[melting point]], such as [[tungsten]].<ref name="StranksEtAl1970">
{{Cite book
| last = Stranks
| first = D. R.
| authorlink =
| coauthors = M. L. Heffernan, K. C. Lee Dow, P. T. McTigue, G. R. A. Withers
| title = Chemistry: A structural view
| publisher = Melbourne University Press
| date = 1970
| location = [[Carlton, Victoria]]
| pages = 5
| url =
| doi =
| id =
| isbn = 0-522-83988-6}}</ref> The sample is held at a large negative potential (1-10 kV) relative to the fluorescent screen. This gives the electric field near the tip apex to be the order of 10<sup>10</sup> V/m which is high enough for [[Field electron emission|field emission]] of electrons to take place. Fig.1 shows the experimental set up for FEM.
[[File:FEM.JPG|thumb|thumb|Fig.1:FEM experimental set-up]]
 
The field emitted electrons travel along the field lines and produce bright and dark patches on the fluorescent screen giving a one-to-one correspondence with the crystal planes of the hemispherical emitter. The emission current varies strongly with the local [[work function]] in accordance with the [[Field electron emission|Fowler-Nordheim equation]]; hence, the FEM image displays the projected work function map of the emitter surface. The closely packed faces have higher work functions than atomically rough regions and thus they show up in the image as dark spots on the brighter background. In short, the work function anisotropy of the crystal planes is mapped onto the screen as intensity variations.
 
The magnification is given by the ratio <math>M=L/R</math>, where <math>R</math> is the tip apex radius and <math>L</math> is the tip-screen distance. Linear magnifications of about 10<sup>5</sup> to 10<sup>6</sup> are attained. The spatial resolution of this technique is of the order of 2 nm and is limited by the momentum of the emitted electrons parallel to the tip surface, which is of the order of the [[Fermi velocity]] of the electron in metal.
 
It is possible to set up an FEM with a probe hole in the phosphor screen and a [[Faraday cup]] collector behind it to collect the current emitted from a single plane. This technique allows the measurement of the variation of work function with orientation for a wide variety of orientations on a single sample. The FEM has also been used to study [[adsorption]] and [[surface diffusion]] processes, making use of the work function change associated with the adsorption process.
 
Field emission requires a very good vacuum, and often, even in [[ultra high vacuum]] (UHV), emission is not due to the clean surface. A typical field emitter needs to be ‘flashed’ to clean it, usually by passing a current through a loop on which it is mounted. After flashing the emission current is high but unstable. The current decays with time and in the process becomes more stable due to the contamination of the tip, either from the vacuum, or more often from diffusion of adsorbed surface species to the tip. Thus the real nature of the FEM tips during use is somewhat unknown.
 
Application of FEM is limited by the materials which can be fabricated in the shape of a sharp tip, can be used in a UHV environment, and can tolerate the high electrostatic fields. For these reasons, [[refractory metals]] with high melting temperature (for e.g. W, Mo, Pt, Ir) are conventional objects for FEM experiments.
 
==See also==
*[[Atom Probe]]
*[[Electron microscope]]
*[[Field ion microscope]]
*[[List of surface analysis methods]]
 
==References==
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{{refbegin}}
* 2. K.Oura, V.G.Lifshits, A.ASaranin, A.V.Zotov and M.Katayama, Surface Science – An Introduction, (Springer-Verlag Berlin Heidelberg 2003).
* 3. John B. Hudson, Surface Science – An Introduction, (BUTTERWORTH-Heinemann 1992).
{{refend}}
 
[[Category:Microscopes]]
[[Category:Scientific techniques]]

Latest revision as of 14:40, 11 December 2014

Hvis du ønsker å bygge et gen sett basert på en bil dynamo din beste (og minst kostbare) er en enkelt ledning Chevrolet. De eldre kjører ca sixty three ampere. De kan bygges om til å produsere høyere ampere, adult men du kan får problemer med overoppheting. S'il ne te plat additionally (pub terrible), enlves le. Il n'y en pas de publicit kraft :) Je ne vais pas Publier notre korrespondanse. J'ai ton write-up d'il y en trois mois. Nunca qualquer c pia vendendo sapatos ou talvez qualquer outra Coisa. Artigos de Venda deve ser retirado o cartaz especial banido. N o um perguntando para decidir sobre o cal larm.

Ce quatrime tome se lit d'une traite! J'ai dj fait l'loge de ses nombreuses qualits, je le dis, je le rpte, cette srie de Nancy Springer est une foredrag prcieuse et kvasi uunnværlig, pas seulement pour les supporters de Sherlock Holmes, mais aussi pour les amatører d ' intriger policires sur toile historique. L'ambiance est, contrairement aux Histoires de Conan Doyle, beaucoup pluss fminine. Porte par la forteller de la petite soeur fiktiv du grand dtective, la srie dcrit l'injuste tilstand du sexe dit faible.

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